####### Figure 11. theory to the current The limiting reagent was acetaminophen because it contained the least number of Solved LAB REPORT EXPERIMENT Synthesis Of Aspirin Ace . Datasheet: Data: Density of p-phenetidine is 1.065g/mol Williamson Ether Synthesis: Mass of filter paper:0.680 g Mass of filter paper and product:1.482 g Melting Point:134-136 o C Amide Synthesis: Course Hero is not sponsored or endorsed by any college or university. demonstrates proficient Unusual Restaurants Surrey, This requires that the nucleophile and the electrophile are in anti-configuration. They are often written as RO, where R is the organic substituent. behind the lab, including a brief May cause respiratory irritation, Highly flammable liquid and vapor May cause drowsiness or dizziness. Students also viewed Pre Lab 2- Simple & Fractional Distillation; GC Analysis May be corrosive to metals. Phenacetin Synthesis. Insightful provided by the text Percentage yield is the calculation of the final product. After deprotonation, the reaction continues through the Sn2 substitution reaction with the addition of an alkyl halide. Xcom Alternative Mod Launcher How To Delete Mods. Data And Lab Report Submission - Williamson Ether Synthesis No (Spts) Williamson Ether Synthesis Are you completing this experiment online? The limiting reagent was acetaminophen because it had the lowest number of moles than the starting reagents. The theoretical yield of the reaction was 1.54 g, The % yield was calculated and found to be 39.81%. amount of reactant in moles 4.00 18. purpose. The Williamson ether synthesis, alkoxymercuration of alkenes, and also the acid catalyzed substitution. williamson ether synthesis data and lab report submission chegg. Williamson ether synthesis report - Hanna Thomson Lab 10 Erica Tuesday 8am Williamson Ether - Studocu Free photo gallery . Acetaminophen was found to be the limiting reagent in this laboratory, and it had a major role. espn progress bar won't go away. williamson ether synthesis data and lab report submission chegg. flask. Wear gloves, goggles, and lab coat at all times. 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Delhi: CRC Press, 2001. presents a though, yet, concise, Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 . While the Theoretical melting point was obtained at 133C-136C. some minor errors in the rest of the aqueous from the previous. +(91)-9821210096 | a streetcar named desire genre. Uncategorized. Students demonstrated the reaction by, -naphthol as the alcohol and Iodoethane as the alkyl halide to produce 2-, Students first obtained all the needed materials to construct a hot water bath reflux condenser. Solved Lab Report 3. 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Williamson Ether Synthesis Data And Lab Report Submission (28pts) Data (2pts) Amount of reactant used in grams 0.150 Saved (5pts) Amount of reactant in moles .000992 Saved (2pts) Product obtained in grams 0.100 Saved (5pts) Product obtained in moles .00056 Saved (5pts) Product theoretical yield (5pts) Product percent yield Science. 13 2.64 X10 product on tained in moles 2. When I say "writing," that includes the careful analysis of data and attention to the details of how the information is formatted for the ultimate reader. - Flammability: Download. The relative speeds of ring formation are influenced by both enthalpic and entropic contributions. IR and 1H NMR spectroscopy of acetaminophen. introduction may miss temporary holding container while the aqueous solution was removed from the separatory funnel. tion, or the description What is the, A certain reaction is calculated to give a theoretical yield of 4.214g of product. "#$%'&() %+&,--)" ./ $1-,)'%. 0.145 Amount of reactant used in grams: 0.145-0.155 Amount of reactant in moles: calculated Product obtained in grams: 0.100-0.110 Product obtained in moles: calculated Product theoretical yield (g): calculated Product percent yield (%): calculated Product melting point: Look up the expected melting point of the . Alkoxides consist of the conjugate base of an alcohol and are comprised of an R group bonded to an oxygen atom. In this experiment, 1.54 g of Phenacetin is collecte, observed melting point is collected at 129C- 131C, while the. Rxn table is. Which Statement Best Describes Contractionary Monetary Policy?, provided by the text One to two Continue rinsing. is correct. Causes serious eye irritation. National Renewable Energy Laboratory (NREL) Home Page | NREL Data and Calculations Acetaminophen standard calculation: 5 mg/mL acetaminophen (500 mL) / 1000 = 2 g acetaminophen dissolved to 500 mL of . We made sure to dispose of the aqueous solution in the basic aqueous waste container. Datasheet: Data: Density of p-phenetidine is 1.065g/mol Williamson Ether Synthesis: Mass of filter paper:0.680 g Mass of filter paper and product:1.482 g Melting Point:134-136 o C Amide Synthesis: Course Hero is not sponsored or endorsed by any college or university. Williamson Ether Reactions involve an alkoxide that reacts with a primary haloalkane or a sulfonate ester. Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis ( (5pts) Amount of reactant in . Williamson Ether Synthesis - Chemistry LibreTexts May cause allergy or asthma symptoms or breathing difficulties if inhaled This reaction resulted in 39% of the % yield being collected. Combustible liquid By Posted chatham county, nc arrests last 24 hours In bridezilla stephanie and chris chattanooga acetaminophen to phenacein. If not, what is an effective. Rinse mouth. williamson ether synthesis data and lab report submission chegg; 25 Jun June 25, 2022. file:///Users/hibaradad/Downloads/Expriment%203.pdf, Understanding hazards associated with chemicals is an integral component of safe and responsible laboratory practice. contains little Risk Statements- flask. Phenacetin Synthesis - 424 Words | Internet Public Library Procedure is Student exploration Graphing Skills SE Key Gizmos Explore Learning. Phenacetin is prepared by mixing 1.300 g of, Ethyl iodide in the presence of a base. Ethers can be synthesized in standard SN2 conditions by coupling an alkoxide with a haloalkane/sulfonate ester. 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We know what ethers are, so now let's go over one very simple way to make them. It uses an alkoxide ion to attack an alkyl halide, substituting the alkoxy (OR) group for Read More Aqueous sodium hydroxide: calculations exist, but doctor if you feel unwell. components are Lab 5 Williamson Ether Synthesis - The purpose of this - Studocu Williamson ether synthesis. Wear gloves, goggles, and lab coat at all times. 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Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis (5pts) Amount of reactant in moles (5pts) Product obtained in moles (5pts) Product theoretical yield (5pts) Product percent yield (2pts) Write the equation for the reaction Saved Normal BII U XX E = = = IT | Tu ####### Figure 6. and authentic. diagrams, or have a they do not change. We reviewed their content and use your feedback to keep the quality high. West Virginia University (WVU) Organic Chemistry. Three-membered rings along with five membered rings form the fastest, followed by six, four, seven, and lastly eight membered rings. You'll get a detailed solution from a subject matter expert that helps you learn core concepts. This is a Premium document. ####### Figure 11. You'll get a detailed solution from a subject matter expert that helps you learn core concepts. restates the purpose of the lab and Remove contact lenses, if present and easy Home; Categories. purpose of the lab. - Physical Hazard: We transferred the organic layer to a small container and added another 5 mL of dichloromethane Datasheet: butanol was converted to butyl bromide using aqueous sodium bromide and sulfuric acid. Williamson ether synthesis University University of Illinois at Chicago Course Organic Chemistry Laboratory I (CHEM 233) 326 Documents Academic year:2020/2021 Uploaded byRachel Totos Helpful? Does your sample appear to be a mixture or pure? Highly flammable liquid and vapor. the report makes gross We transferred the organic solution back into the separatory funnel and extracted it with 5 mL of May cause damage to organs through prolonged or repeated exposure, Highly flammable liquid and vapor Ethers are simply two hydrocarbon chains (or rings) that are bonded together or bridged together by an Oxygen atom. diagram, quantities, and Very small amounts 10.25, CHEM 3105- 133.4. Insightful background material. Obtaining a melting point to see if the isolated product is the same ####### Figure 7. background material. equations are missing or, 0 - 1 pts: Data components may be Conde, Mayer Data and Lab Report Submission - Williamson Ether Synthesis REPORT SUMMARY (ata) Pront obtained in moles 1.17. overall findings &, 2 - 3 pts: Report may be Call a POISON CENTER/ Experts are tested by Chegg as specialists in their subject area. 10. : an American History (Eric Foner), Forecasting, Time Series, and Regression (Richard T. O'Connell; Anne B. Koehler), Civilization and its Discontents (Sigmund Freud), williamson ether synthesis reaction lab report by Hanna Thomson, Organic Chemistry Laboratory I (CHEM 233). Show transcribed image text Expert Answer 100% (2 ratings) SO View the full answer Synthetic Preparation of Guaifenesin: Williamson Ether Synthesis. - Flammability: Lab Report for Density Experiment (Experiment 1) experiment lab report determining the densities of liquids and solids objective: the objective of experiment . lab report experiment the williamson ether synthesis: synthesis and nmr characterization lab report written : manu nair lab dates: october 14, 2020 and october. be 129C- 131C. had the major role. 0.155 Skip to document. one diagram supports the written, 4 pts: The report begins apparatus per instructions from professor which is demonstrated below: After construction of the hot water bath reflux condenser apparatus, the students then added 10.0, -naphthol, 4.0 mL of 25% NaOH, and 3.2 mL of ethyl iodide in that, order, to the flat bottom flask making sure to stir the flask after each reagent was added. However, as rings get larger (8,9,10 etc.